Pickling, passivation and removing iron contamination with nitric acid ASTM A – Practice for Cleaning, Descaling and Passivating of Stainless Steel Parts, . I currently need to passivate a partly electropolished L stainless steel The passivation procedure I intend following, in general, ASTM ASTM A [link is to . Delstar Metal Finishing maintains high standards in stainless steel passivation, meeting the ASTM A standards. ASTM A passivation standards include.
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I think you may be thinking of ammonium hydrogen difluoride which is often used in place of hydrofluoric acid in pickle solutions. Stainless steels asgm be passivated unless the steel surface is clean and free from contamination and scale from welding operations. The standard notes that the high carbon martensitic stainless steels, such as C, are not suitable for acid passivation as they can be attacked or be subject to hydrogen embrittlement.
Tests with acceptance criteria to demonstrate that the passivation procedures have been successful are listed in 7. Depending on the application, chemical descaling acid pickling as described in 5. Others, such as food-handling, pharmaceutical, aerospace, and certain nuclear applications, may require extremely high levels of cleanness, including removal of all detectable residual chemical films and contaminants that are invisible to ordinary inspection methods.
I believe you must pickle the spools with an acid which contains fluoride in some form — often a standard nitric-hydrofluoric pickling acid or pickling paste, and follow this either with electropolishing or with nitric acid passivation or citric acid passivation to the standards discussed above.
On the other hand, some of the practices may be applicable for these purposes.
All information presented is for general reference and does not represent a professional opinion nor the policy of an author’s employer. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Methods are described for the detection of free iron and transparent chemical and oily deposits.
It is informational only and not an official part of the standard; x380 full text of the standard itself must be referred to for its use and application. Our facility is capable of handling a wide variety of projects, whether you need ATM A standards or a different type of finishing.
Passivvation inspection shall be performed by solvent-ring test, black light inspection, atomizer test, and ferroxyl test. This practice covers the standard recommendations and precautions for cleaning, descaling, and passivating of pasisvation stainless steel parts, assemblies, equipment, and installed systems.
It is also quite out of date and needs to be updated. In order to avoid ambiguity in the setting of requirements, it passivatioh be necessary for the purchaser to define precisely the intended meaning of passivation. Some of the various meanings associated with the term passivation that are in common usage include the following:.
ASTM A – Stainless Steel Passivation by Keystone Finishing
Give us a call or visit our contact page to request a quote for your project today! It was at one time considered that an oxidizing treatment was necessary to establish this passive metal oxide film, but asm is now accepted that this film will form spontaneously in an oxygen-containing environment providing that the surface has been xstm cleaned or descaled.
Pickling, passivation and removing iron contamination with nitric acid Passivation treatments are sometimes specified, but it is important to consider whether asttm is strictly necessary or not. Visual inspection; wipe tests; residual pattern; water-break test; free iron test such as water-wetting or drying; high-humidity test; and copper sulfate test. Combining values from the two systems may aetm in non-conformance with the standard. This standard covers both nitric and citric acid treatments.
I am not sure exactly what you want to do, but the citric formulations can give you increased performance over the old nitric formulations.
It’s not possible to diagnose a finishing problem or the hazards of an operation via these pages. Consideration shall be given in the design of parts, equipment, and systems that will require cleaning to minimize the presence of areas in which dirt, or cleaning solutions might become trapped, and to provide for effective circulation and removal of cleaning solutions.
Scales shall be removed through chemical descaling, acid pickling, and mechanical descaling. I agree with Lee that what you are proposing should not be a problem lassivation the EP’d surfaces. Passivation treatments are sometimes specified, but it is important to consider whether this is strictly necessary or not.
Lee Kremer Stellar Solutions, Inc. Although they apply primarily to materials in the composition ranges of the austenitic, ferritic, martensitic, and duplex stainless steels, the practices described may also be useful for cleaning other metals if due consideration is given to corrosion and possible metallurgical effects. Citric acid is a less hazardous method and has environmental benefits in terms of ‘NOx’ fume emission and waste acid disposal.
Link to Active This link will always route to the current Active version of the standard. The treatments are then defined by the process classes.
Range C Time mins. Our passivatoin are capable asrm handling both large and small parts. This would attack electro-polished surfaces and is not the kindest way to treat them. Unlike ASTM A, s380 standard does not require specific solutions for particular stainless steel grades or types, although 3 specific treatments are identified. This ensures that the surface of the workpiece is free of scale and contaminates.
Passivation of 316L SS per ASTM A380
This formula should not hurt your electropolished surfaces. The selection of procedures from this practice to be applied to the parts may be specified upon agreement between the supplier and the purchaser.
Stainless steels are designed to naturally self-passivate whenever a clean surface is exposed to an environment that can provide enough oxygen to form the chromium rich oxide passivztion layer, on which the corrosion resistance of these alloys depends.
In the case of classes C3 and C4, a two step process is defined, with a clean water rinse between the two steps, shown in the table below. Citric acid treatments can also be considered as an alternative to nitric acid as both provide the oxidising conditions necessary for passivation. Specific treatments are however also specified. Materials shall be precleaned. Some of the various meanings associated with the term passivation that are in common usage include the following: The degree of cleanness required on a passivatuon depends on the application.
Visual inspection is suitable for the detection of gross contamination, scale, rust, and particulates, but may not reveal the presence of thin films of oil or residual chemical films.
Although cannot see the reason obviously myself? Passivation is a process passovation removes exogenous iron or iron compounds from the surface of the stainless steel alloy.
I currently need to passivate a partly electropolished Aztm stainless steel process system. If the piping system is already assembled, there are service companies which specialize in on-site projects of this sort, like Astropak.